Burette Accuracy: Class A vs Class B, Reading Errors, and Calibration
Pick by the job, not by habit
Burette vs pipette, side by side
Class A vs Class B — what the tolerance numbers mean in practice
ISO 385 defines two accuracy classes for burettes. Class A has the tighter tolerance: a 50 mL Class A burette carries ±0.05 mL absolute error. Class B allows twice that: ±0.10 mL. For a single titration that difference is small; across hundreds of titrations in a QC or regulated environment it accumulates into a systematic offset. Use Class A wherever the result feeds a calculation or a compliance record.
The volume-range accuracy trap
A burette's tolerance is stated as an absolute value (±0.05 mL), not a percentage. At 50 mL delivery that is 0.1 % relative error — excellent. At 5 mL delivery it is 1 % relative error — ten times worse. At 2 mL it is 2.5 %. The burette did not change; the maths did. For small deliveries, a volumetric pipette or a smaller-range burette gives better relative accuracy.
Three reading errors that cost accuracy
- Parallax at the meniscus. The eye must be exactly level with the bottom of the meniscus. Reading from above gives a lower reading; from below, higher — a consistent systematic offset every titration.
- Not rinsing with titrant before use. Rinsing with distilled water and then filling with titrant leaves a dilution layer on the glass walls. Rinse the burette two or three times with the titrant itself before starting.
- Ignoring the stopcock dead volume. The volume between the stopcock and the tip is not on the scale. A drop hanging on the tip at the endpoint is not accounted for. Touch the tip to the vessel wall to include it in the delivery.
